r-2,c-6-Bis(3-methoxy­phen­yl)-t-3,t-5-dimethyl­piperidin-4-one

نویسندگان

  • P. Parthiban
  • V. Ramkumar
  • Nanjundan Ashok Kumar
  • Jong Su Kim
  • Yeon Tae Jeong
چکیده

In the title compound, C(21)H(25)NO(3), the piperidinone ring adopts a chair conformation with an equatorial orientation of all substituents; the 3-methoxy-phenyl groups make a dihedral angle of 60.26 (15)°. The carbonyl group O atom is disordered over two positions in a 0.643 (3):0.357 (3) ratio. The crystal structure is stabilized by N-H⋯O and C-H⋯O hydrogen bonding.

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منابع مشابه

r-2,c-6-Bis(2-methoxy­phen­yl)-t-3,t-5-dimethyl­piperidin-4-one acetic acid solvate

In the title compound, C(21)H(25)NO(3)·C(2)H(4)O(2), the piperidone ring adopts a chair conformation. The two meth-oxy groups are nearly coplanar with the aromatic rings to which they are attached. The dihedral angle between the two aromatic rings is 60.9 (2)°. There are two short intra-molecular N-H⋯O contacts. The crystal packing is stabilized by inter-molecular O-H⋯N and C-H⋯O inter-actions.

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1-Dichloro­acetyl-r-2,c-6-bis­(4-methoxy­phen­yl)-t-3,t-5-dimethyl­piperidin-4-one

In the title compound, C(23)H(25)Cl(2)NO(4), the piperidine ring adopts a distorted boat conformation. The dihedral angle between the benzene rings is 54.8 (1)°. In the crystal, the mol-ecules are linked into a two-dimensional network parallel to the ab plane by C-H⋯O hydrogen bonds.

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r-2,c-6-Bis(4-methoxy­phen­yl)-c-3,t-3-dimethyl­piperidin-4-one

The asymmetric unit of the title compound, C(21)H(25)NO(3), contains two crystallographically independent mol-ecules (A and B). In both mol-ecules, the piperidine ring adopts a chair conformation, with the methoxy-phenyl rings attached equatorially. The dihedral angle between the two benzene rings in mol-ecule A is 73.79 (8)°; the corresponding value in mol-ecule B is 77.71 (8)°. The mol-ecules...

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1-Dichloro­acetyl-r-2,c-6-bis­(4-methoxy­phen­yl)-c-3,t-3-dimethyl­piperidin-4-one

In the title compound, C(23)H(25)Cl(2)NO(4), the piperidine ring adopts a distorted boat conformation. Inversion-related mol-ecules are linked into centrosymmetric R(2) (2)(16) dimers by paired C-H⋯O hydrogen bonds, and the dimers are connected via C-H⋯O hydrogen bonds into a chain running along [101].

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1-Formyl-r-2,c-6-bis­(4-methoxy­phen­yl)-c-3,t-3-dimethyl­piperidin-4-one

In the title compound, C(22)H(25)NO(4), the piperidine ring adopts a distorted boat conformation. The two benzene rings are approximately perpendicular to each other, making a dihedral angle of 86.2 (8)°. The crystal packing is stabilized by C-H⋯O and C-H⋯π inter-actions.

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عنوان ژورنال:

دوره 64  شماره 

صفحات  -

تاریخ انتشار 2008